本品为天南星科植物天南星Arisaemaerubescens(Wall、)Schott、异叶天南星ArisaemaheterophyllumBl、或东北天南星ArisaemaamurenseMaxim、的干燥块茎。秋、冬二季茎叶枯萎时采挖,除去须根及外皮,干燥。
【性状】本品呈扁球形,高1~2cm,直径1、5~6、5cm。表面类白色或淡棕色,较光滑,顶端有凹陷的茎痕,周围有麻点状根痕,有的块茎周边有小扁球状侧芽。质坚硬,不易破碎,断面不平坦,白色,粉性。气微辛,味麻辣。
【鉴别】(1)本品粉末类白色。淀粉粒以单粒为主,圆球形或长圆形,直径2~17μm,脐点点状、裂缝状,大粒层纹隐约可见;复粒少数,由2~12分粒组成。草酸钙针晶散在或成束存在于黏液细胞中,长63~131μm。草酸钙方晶多见于导管旁的薄壁细胞中,直径3~20μm。
(2)取本品粉末5g,加60%乙醇50ml,超声处理45分钟,滤过,滤液置水浴上挥尽乙醇,加于AB-8型大孔吸附树脂柱(内径为1cm,柱高为10cm)上,以水50ml洗脱,弃去水液,再用30%乙醇50ml洗脱,收集洗脱液,蒸干,残渣加乙醇1ml使溶解,离心,取上清液作为供试品溶液。另取天南星对照药材5g,同法制成对照药材溶液。照薄层色谱法(通则0502)试验,吸取上述两种溶液各6μl,分别点于同一硅胶G薄层板上,以乙醇-吡啶-浓氨试液-水(8∶3∶3∶2)为展开剂,展开,取出,晾干,喷以5%氢氧化钾甲醇溶液,分别置日光和紫外光灯(365nm)下检视。供试品色谱中,在与对照药材色谱相应的位置上,显相同颜色的斑点。
【检查】水分不得过15、0%(通则0832第二法)。
总灰分不得过5、0%(通则2302)。
【浸出物】照醇溶性浸出物测定法(通则2201)项下的热浸法测定,用稀乙醇作溶剂,不得少于9、0%。
【含量测定】对照品溶液的制备取芹菜素对照品适量,精密称定,加60%乙醇制成每1ml含12μg的溶液,即得。
标准曲线的制备精密量取对照品溶液1ml、2ml、3ml、4ml、5ml,分别置10ml量瓶中,各加60%乙醇至5ml,加1%三乙胺溶液至刻度,摇匀,以相应的试剂为空白,照紫外-可见分光光度法(通则0401),在400nm的波长处测定吸光度,以吸光度为纵坐标,浓度为横坐标,绘制标准曲线。
测定法取本品粉末(过四号筛)约0、6g,精密称定,置具塞锥形瓶中,精密加入60%乙醇50ml,密塞,称定重量,超声处理(功率250W,频率40kHz)45分钟,放冷,再称定重量,用60%乙醇补足减失的重量,摇匀,滤过。精密量取续滤液5ml,置10ml量瓶中,照标准曲线的制备项下的方法,自“加1%三乙胺溶液”起,依法测定吸光度,从标准曲线上读出供试品溶液中含芹菜素的重量,计算,即得。
本品按干燥品计算,含总黄酮以芹菜素(C15H10O5)计,不得少于0、050%。
饮片
【炮制】生天南星除去杂质,洗净,干燥。
【性状】【鉴别】【检查】【浸出物】【含量测定】同药材。
【性味与归经】苦、辛,温;有毒。归肺、肝、脾经。
【功能与主治】散结消肿。外用治痈肿,蛇虫咬伤。
【用法与用量】外用生品适量,研末以醋或酒调敷患处。
【注意】孕妇慎用;生品内服宜慎。
【贮藏】置通风干燥处,防霉、防蛀。
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